| 李飒英.微纳米硼酸镍材料的制备及表征[J].陕西学前师范学院学报,2016,32(9):146-149 |
| 微纳米硼酸镍材料的制备及表征 |
| The Preparation and Characterization of Micro/nano Nickel Borate Materials |
| 投稿时间：2015-12-28 修订日期：2016-03-24 |
| DOI：10.11995/j.issn.2095-770X.2016.09.033 |
| 中文关键词: 微纳米材料 形貌 溶胶-凝胶法 表征 |
| 英文关键词: micro/nano material morphogy Sol-Gel method characterization |
| 基金项目: |
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| 摘要点击次数: 1566 |
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| 中文摘要: |
| 采用溶胶-凝胶法以醋酸镍、氯化镍、硼酸和表面活性剂为主要原料，通过改变反应物的比例和种类、反应温度、反应时间以及表面活性剂的用量和种类等条件，制备出了片状、粒状和棒状三种不同形貌的微纳米硼酸镍。在此基础上，对新合成出来的微纳米硼酸镍进行了X射线的粉末衍射 (XRD)、红外光谱(FT-IR)、扫描电子显微镜(SEM)等多种表征。 |
| 英文摘要: |
| Three different shape micro/nano nickel borate such as flake, granular, and rod has been synthesized with nickel acetate, nickel chloride, boric acid and surfactant as the main raw materials under the Sol-Gel conditions, by changing the ratio of reactants and kinds, temperature, time and the amount of surfactant, etc. Meanwhile, the synthetic materials characterized by X-ray powder diffraction (XRD), infrared spectroscopy (FT-IR), scanning electron microscope (SEM). |
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